GUTMANN BRAGA PDF

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Jump to site search. DR-UV-vis and XPS demonstrate that the oxidation state and the Rh—Rh single bond in the dirhodium node are maintained during the ligand substitution process.

Heterogeneous self-supported dirhodium II catalysts with high catalytic efficiency in cyclopropanation — a structural study.

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Residual trifluoroacetate species are investigated by quantitative 19 F MAS NMR which further reflects the configuration of trifluoroacetate in the obtained Rh 2 -bdc Tfand defects in the structure.

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Heterogeneous self-supported dirhodium II catalysts with high catalytic efficiency in cyclopropanation — a structural study J. The catalysts show similar catalytic efficiency as the homogeneous catalyst in the model cyclopropanation between ethyl diazoacetate EDA and styrene. The individual lamellae of the dirhodium-bdc frameworks are stacked as parallel sheets, which are randomly oriented or slightly ordered. Please enable JavaScript to access the full features of the site or access our non-JavaScript page.

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The stability and reusability of the catalysts are verified by TG-DTA measurements and leaching tests. Catalytically active dirhodium sheet-like coordination polymers are synthesized from their precursors via gutmnan exchange. The article was received on 26 Apraccepted on 20 Sep and first published on 21 Sep Supplementary information PDF K. For reproduction of material from PCCP: Authors contributing to RSC publications journal articles, books or book chapters do not need to formally request permission to reproduce material contained in this article provided that the correct acknowledgement is given with the reproduced material.

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